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Transfer the cleared supernatant to an IODOGEN-treated 1.5mL microcentrifuge tube and place m a fume hood. 4. Add 500 pC1 of sodium 125iodide (5 pL of the stock solution of sodium ‘25iodide at 100 mCi/mL in NaOH, pH 7-l l), close the cap, and agitate intermittently for 5 min. 5.

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Samples were taken immediately after preparation (day 0) and on days 1, 2, 3, 6, 13, 20, and 27 for analysis with a stability-indicating high-performance liquid chromatography assay in order to determine solution concentration. Stability was defined as retention of at least 90% of the initial drug concentration.

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HPLC. This vial delivers maximum sample capacity (~1 mL) with minimum residual volume (~9 μL). Waters Maximum Recovery Vial Specifically designed for the bottom draw-port needle of the Waters ACQUITY UPLC and Alliance HT HPLC Systems. This vial delivers maximum sample capacity (~1.5 mL) with minimum residual volume. The 9 mm cap

Jun 22, 2012 · 3.Ion-pair chromatography•It is a form of chromatography in which ions in solution can be "paired"or neutralized and separated as an ion pair on a reversed-phase column.•Ion-pairing agents are usually ionic compounds that contain ahydrocarbon chain that imparts a certain hydrophobacity so that the ionpair can be retained on a reversed-phase

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