Exploring the Impact of Vial Dimension on Sample Dispersion and Peak Efficiency in Autosamplers

Jul 25, 2014 · In order to maximize data accuracy, the sample dispersion through a single frit was measured from four independent methods: (1) plate height subtraction, (2) peak capacity versus efficiency plot, (3) flow reversal, and (4) direct measurement. Frit dispersion increases non-linearly with increasing flow rate.

This application note will detail the origins and measurement of extra-column dispersion and demonstrate the impact that extra-column dispersion has on the efficiency of SEC separations. We will conclude by summarizing useful considerations in the selection of an SEC particle size and column geometry for protein separations. EXPERIMENTAL

Once you have found an appropriate dispersant to wet the sample, you then need to assess the state of dispersion of the sample in the instrument. We call this process a dispersion titration, which generally involves three steps: 1. A set of repeat measurements to assess the effect of stirring the sample 2.

Feb 5, 2015 · Polypropylene vials are suitable for biological applications and for applications involving samples with high metal content, such as ion chromatography, AA, or ICP-MS. Because many Aijiren autosamplers use a robotic arm to grip vials by the neck, it is important the vial is the correct size to prevent them being dropped and samples lost.

Jan 31, 2022 · For more routine analysis, certified vials will probably be an unnecessary expense. You may require amber vials for light sensitive sample to maximise lifetime. Vial inserts may help to inject very small volumes of sample. However, many labs like to use the same vial for all HPLC use and not have to choose a vial for each analysis.

Dec 19, 2022 · The dark ages of sample vials. Certified vials have been around for the better part of 20 years. Some of you may remember the olden days when it was an adventure to choose the right vial for an application. Autosamplers, or sample managers of the day used different vial formats, depending on the manufacturer.

Deactivated Clear Glass 12 x 32 mm Screw Neck Vial with Cap and Preslit PTFE/Silicone Septum, 2 mL Volume, 100/pk. This item is not available for sale. Contact Waters for more information. SKU: 186000327C. LCGC Certified Clear Glass 12 x 32 mm Screw Neck Vial, Max Recovery, with Cap and Preslit PTFE/Silicone Septum, 1.5 mL Volume, 100/pk.

Aug 1, 2019 · This installment is the second of a series of four white papers on high-performance liquid chromatography (HPLC) modules focusing on pumps, autosamplers, ultraviolet (UV) detectors, and

specified volume of reagent or solvent from a specified vial, and inject it together with the sample, or to mix it with the sample inside the needle. Using this function, a specified volume of reagent (or solvent) from a specified vial can be injected together with the sample (Fig. 1). 1. Co-Injection Function

VWR® Ion Chromatography (IC) Vials are compatible with Dionex® and Metrohm-Peak® Autosamplers.Vials are available in all capacities, materials like plastic vials or glass vials, and in a variety of colors to meet any collection, storage, or analysis need. Tailor vessels for specific media with various translucent manufacturing and different sterility options for precise test results. Choose

sampling needle to the respective vial coordinates. The dimensions of autosampler vials vary. Most autosamplers are equipped w ith trays that use 12x32mm vial configurations but some like the Waters Wisp require a 15x45mm configuration. Consult your autosam pler’s operating manual or manufacturer to determine the vial dimensions required

Jan 31, 2018 · The Shimadzu Nexera X2 ultra high-performance liquid chromatography (UHPLC) system offers unsurpassed chromatographic efficiency, sensitivity, resolution, stability, and reliability. The Nexera X2 is a truly flexible design that expands to tackle a broad range of UHPLC applications. Nexera X2 covers a broad range of UHPLC application demands.

May 17, 2021 · During the 400‑bar era of liquid chromatography (LC) that lasted through the mid‑2000s, instrument manufacturers worked to adjust the dimensions of component parts, including connecting tubing and detector elements, so that the impact of dispersion of the analyte zone outside of the column was manageable, and did not seriously affect

46 and B) sample is drawn from a vial by an automated syringe and subsequently transferred to a 47 sample loop, in either a pushed loop mode (as illustrated in Fig. 2A-B) or pulled through the needle 48 directly into the sample loop (pulled loop design) [4]. During the sample loading (“load” position),